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. 2011 Nov 5;67(Pt 12):m1695–m1696. doi: 10.1107/S1600536811046150
x y z Uiso*/Ueq Occ. (<1)
Rh1 0 0.5 0.5 0.01620 (12)
Rh2 0 0 0 0.01681 (12)
P1 0.17881 (11) 0.45129 (8) 0.59018 (4) 0.0169 (2)
P2 0.19028 (11) 0.15093 (8) −0.03218 (4) 0.0169 (2)
C1 −0.0559 (14) 0.3657 (10) 0.4714 (6) 0.034 (3) 0.5
C2 0.3688 (4) 0.5602 (3) 0.62055 (16) 0.0169 (8)
C3 0.4759 (4) 0.6069 (3) 0.57726 (17) 0.0196 (8)
H023 0.4495 0.579 0.5336 0.023*
C4 0.6194 (4) 0.6927 (3) 0.59619 (18) 0.0210 (8)
H035 0.6927 0.7215 0.5663 0.025*
C5 0.6553 (5) 0.7363 (3) 0.65925 (19) 0.0228 (8)
C6 0.5486 (5) 0.6916 (3) 0.70302 (18) 0.0230 (8)
H030 0.5727 0.7214 0.7462 0.028*
C7 0.4080 (4) 0.6042 (3) 0.68391 (17) 0.0198 (8)
H047 0.3372 0.5738 0.7143 0.024*
C8 0.8885 (6) 0.8790 (4) 0.6380 (2) 0.0418 (12)
H04A 0.9481 0.8272 0.6187 0.063*
H04B 0.9769 0.9412 0.6604 0.063*
H04C 0.8091 0.9069 0.604 0.063*
C9 0.2703 (4) 0.3274 (3) 0.58447 (16) 0.0179 (8)
C10 0.4508 (4) 0.3317 (3) 0.58604 (16) 0.0184 (8)
H048 0.5295 0.4016 0.5905 0.022*
C11 0.5171 (5) 0.2356 (3) 0.58120 (17) 0.0221 (8)
H036 0.64 0.2404 0.5823 0.027*
C12 0.4043 (5) 0.1327 (3) 0.57470 (17) 0.0220 (8)
C13 0.2238 (5) 0.1265 (3) 0.57155 (18) 0.0233 (8)
H022 0.1452 0.0565 0.5662 0.028*
C14 0.1590 (4) 0.2230 (3) 0.57627 (17) 0.0222 (8)
H046 0.0355 0.2178 0.5739 0.027*
C15 0.3688 (6) −0.0645 (3) 0.5660 (2) 0.0342 (10)
H05J 0.3069 −0.0728 0.6029 0.051*
H05K 0.44 −0.1216 0.5657 0.051*
H05L 0.2822 −0.0724 0.5259 0.051*
C16 0.0517 (4) 0.4249 (3) 0.65485 (16) 0.0174 (8)
C17 0.0822 (4) 0.3493 (3) 0.70175 (17) 0.0212 (8)
H034 0.1791 0.3132 0.7026 0.025*
C18 −0.0271 (4) 0.3261 (3) 0.74719 (17) 0.0210 (8)
H033 −0.0038 0.2751 0.7793 0.025*
C19 −0.1717 (4) 0.3776 (3) 0.74576 (17) 0.0192 (8)
C20 −0.1985 (4) 0.4567 (3) 0.70120 (17) 0.0190 (8)
H043 −0.2924 0.4951 0.7016 0.023*
C21 −0.0880 (4) 0.4794 (3) 0.65610 (17) 0.0197 (8)
H014 −0.1077 0.5333 0.6254 0.024*
C22 −0.4399 (4) 0.3816 (4) 0.78430 (18) 0.0257 (9)
H04D −0.4143 0.4615 0.7948 0.039*
H04E −0.5113 0.3433 0.8143 0.039*
H04F −0.5052 0.3664 0.7401 0.039*
C23 −0.0457 (15) −0.0644 (11) −0.0774 (5) 0.020 (2) 0.5
C24 0.0810 (4) 0.2656 (3) −0.05056 (17) 0.0174 (8)
C25 0.1519 (4) 0.3536 (3) −0.08578 (17) 0.0196 (8)
H037 0.2597 0.353 −0.1006 0.024*
C26 0.0674 (4) 0.4416 (3) −0.09933 (17) 0.0184 (8)
H019 0.1175 0.5006 −0.1232 0.022*
C27 −0.0899 (4) 0.4437 (3) −0.07806 (17) 0.0170 (7)
C28 −0.1621 (4) 0.3576 (3) −0.04193 (17) 0.0195 (8)
H044 −0.2683 0.3594 −0.0262 0.023*
C29 −0.0769 (4) 0.2694 (3) −0.02936 (17) 0.0172 (8)
H017 −0.1276 0.2102 −0.0057 0.021*
C30 −0.1136 (5) 0.6129 (3) −0.12824 (19) 0.0253 (9)
H05D 0.0028 0.6508 −0.1055 0.038*
H05E −0.1928 0.6659 −0.1347 0.038*
H05F −0.102 0.5823 −0.1702 0.038*
C31 0.2855 (4) 0.1317 (3) −0.10391 (17) 0.0172 (8)
C32 0.1737 (4) 0.1092 (3) −0.16402 (17) 0.0196 (8)
H021 0.0512 0.1087 −0.1671 0.023*
C33 0.2403 (5) 0.0879 (3) −0.21875 (18) 0.0239 (9)
H026 0.1636 0.0744 −0.2593 0.029*
C34 0.4202 (5) 0.0860 (3) −0.21482 (18) 0.0225 (8)
C35 0.5329 (4) 0.1102 (3) −0.15605 (17) 0.0207 (8)
H016 0.6556 0.1114 −0.153 0.025*
C36 0.4641 (4) 0.1327 (3) −0.10139 (17) 0.0182 (8)
H041 0.5418 0.1493 −0.0612 0.022*
C37 0.6495 (6) 0.0500 (4) −0.2687 (2) 0.0389 (11)
H05A 0.727 0.1218 −0.2545 0.058*
H05B 0.6674 0.0277 −0.3116 0.058*
H05C 0.6775 −0.0058 −0.2382 0.058*
C38 0.3798 (4) 0.2067 (3) 0.03055 (17) 0.0178 (8)
C39 0.4737 (5) 0.1321 (3) 0.06249 (17) 0.0224 (8)
H031 0.4463 0.0563 0.0479 0.027*
C40 0.6072 (5) 0.1675 (3) 0.11553 (18) 0.0222 (8)
H054 0.6728 0.1167 0.136 0.027*
C41 0.6431 (4) 0.2766 (3) 0.13794 (17) 0.0187 (8)
C42 0.5510 (4) 0.3518 (3) 0.10570 (18) 0.0194 (8)
H018 0.5768 0.4274 0.1207 0.023*
C43 0.4228 (4) 0.3165 (3) 0.05225 (18) 0.0190 (8)
H032 0.3633 0.3686 0.03 0.023*
C44 0.8474 (5) 0.2447 (4) 0.22982 (19) 0.0304 (10)
H05G 0.7578 0.1861 0.2427 0.046*
H05H 0.922 0.2847 0.2684 0.046*
H05I 0.9207 0.2117 0.2047 0.046*
O1 −0.1082 (16) 0.2772 (11) 0.4481 (7) 0.034 (3) 0.5
O2 0.7890 (3) 0.8233 (2) 0.68280 (13) 0.0293 (7)
O3 0.4817 (3) 0.0430 (2) 0.57075 (13) 0.0283 (6)
O4 −0.2777 (3) 0.3427 (2) 0.78963 (12) 0.0237 (6)
O5 −0.085 (2) −0.1068 (14) −0.1294 (5) 0.037 (3) 0.5
O6 −0.1854 (3) 0.5247 (2) −0.09059 (12) 0.0209 (6)
O7 0.4683 (4) 0.0594 (3) −0.27137 (13) 0.0319 (7)
O8 0.7629 (3) 0.3197 (2) 0.19171 (12) 0.0231 (6)
Cl1 −0.0738 (4) 0.3106 (4) 0.4565 (2) 0.0283 (11) 0.5
Cl2 −0.0659 (5) −0.0881 (4) −0.10676 (18) 0.0247 (9) 0.5