| Oxford Diffraction Xcalibur Sapphire3 Gemini ultra diffractometer | 4977 independent reflections |
| Radiation source: Enhance (Mo) X-ray Source | 3050 reflections with I > 2σ(I) |
| graphite | Rint = 0.037 |
| Detector resolution: 15.9149 pixels mm-1 | θmax = 26.4°, θmin = 2.9° |
| ω scans | h = −30→29 |
| Absorption correction: multi-scan (ABSPACK; Oxford Diffraction, 2009) | k = −14→17 |
| Tmin = 0.829, Tmax = 0.868 | l = −14→19 |
| 12270 measured reflections |