| Bruker APEXII CCD diffractometer | 2243 independent reflections |
| Radiation source: fine-focus sealed tube | 1862 reflections with I > 2σ(I) |
| graphite | Rint = 0.019 |
| φ and ω scans | θmax = 25.3°, θmin = 2.4° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −5→5 |
| Tmin = 0.977, Tmax = 0.996 | k = −10→10 |
| 3432 measured reflections | l = −18→18 |