| Bruker SMART CCD area-detector diffractometer | 1113 independent reflections |
| Radiation source: fine-focus sealed tube | 759 reflections with I > 2σ(I) |
| graphite | Rint = 0.046 |
| phi and ω scans | θmax = 25.0°, θmin = 2.9° |
| Absorption correction: multi-scan (SADABS; Bruker, 2007) | h = −16→16 |
| Tmin = 0.956, Tmax = 0.974 | k = −19→7 |
| 4543 measured reflections | l = −6→6 |
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