| Bruker APEXII CCD area-detector diffractometer | 2292 independent reflections |
| Radiation source: fine-focus sealed tube | 1572 reflections with I > 2σ(I) |
| graphite | Rint = 0.030 |
| φ and ω scans | θmax = 25.5°, θmin = 2.6° |
| Absorption correction: multi-scan (SADABS; Bruker, 2001) | h = −9→9 |
| Tmin = 0.969, Tmax = 0.989 | k = −10→10 |
| 4891 measured reflections | l = −11→11 |
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