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. 2011 Nov 25;67(Pt 12):o3414. doi: 10.1107/S1600536811049208
Oxford Diffraction Gemini diffractometer 2548 independent reflections
Radiation source: fine-focus sealed tube 2214 reflections with I > 2σ(I)
graphite Rint = 0.030
ω/2θ scans θmax = 71.1°, θmin = 4.2°
Absorption correction: multi-scan (CrysAlis RED; Oxford Diffraction, 2006) h = −13→15
Tmin = 0.810, Tmax = 0.900 k = −12→12
12046 measured reflections l = −23→25