Oxford Diffraction Gemini diffractometer | 2548 independent reflections |
Radiation source: fine-focus sealed tube | 2214 reflections with I > 2σ(I) |
graphite | Rint = 0.030 |
ω/2θ scans | θmax = 71.1°, θmin = 4.2° |
Absorption correction: multi-scan (CrysAlis RED; Oxford Diffraction, 2006) | h = −13→15 |
Tmin = 0.810, Tmax = 0.900 | k = −12→12 |
12046 measured reflections | l = −23→25 |