Bruker SMART APEXII CCD diffractometer | 6681 independent reflections |
Radiation source: fine-focus sealed tube | 5130 reflections with I > 2σ(I) |
graphite | Rint = 0.039 |
φ and ω scans | θmax = 30.0°, θmin = 1.9° |
Absorption correction: multi-scan (SADABS; Bruker, 2009) | h = −13→14 |
Tmin = 0.896, Tmax = 0.968 | k = −30→28 |
26235 measured reflections | l = −16→13 |