Bruker SMART APEXII area-detector diffractometer | 4990 independent reflections |
Radiation source: fine-focus sealed tube | 4981 reflections with I > 2σ(I) |
graphite | Rint = 0.025 |
0.50° ω and 0.5 ° φ scans | θmax = 71.7°, θmin = 4.4° |
Absorption correction: multi-scan (SADABS; Bruker, 2007) | h = −15→14 |
Tmin = 0.352, Tmax = 0.403 | k = −15→16 |
34598 measured reflections | l = −18→17 |