| Bruker APEXII CCD diffractometer | 1786 independent reflections |
| Radiation source: fine-focus sealed tube | 1313 reflections with I > 2σ(I) |
| graphite | Rint = 0.040 |
| φ and ω scans | θmax = 28.0°, θmin = 2.0° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −7→7 |
| Tmin = 0.974, Tmax = 0.984 | k = −14→16 |
| 7948 measured reflections | l = −23→20 |