| Rigaku R-AXIS RAPID IP diffractometer | 2988 independent reflections |
| Radiation source: fine-focus sealed tube | 2379 reflections with I > 2σ(I) |
| graphite | Rint = 0.028 |
| Detector resolution: 10.0 pixels mm-1 | θmax = 25.2°, θmin = 3.3° |
| ω scans | h = −5→7 |
| Absorption correction: multi-scan (ABSCOR; Higashi, 1995) | k = −14→11 |
| Tmin = 0.56, Tmax = 0.72 | l = −14→14 |
| 5637 measured reflections |