| Bruker APEXII CCD area detector diffractometer | 2252 independent reflections |
| Radiation source: fine-focus sealed tube | 2169 reflections with I > 2σ(I) |
| graphite | Rint = 0.040 |
| φ and ω scans | θmax = 18.6°, θmin = 1.0° |
| Absorption correction: multi-scan (SADABS; Bruker, 2009) | h = −6→6 |
| Tmin = 0.690, Tmax = 0.744 | k = −8→8 |
| 9141 measured reflections | l = −19→19 |