| Bruker APEXII CCD diffractometer | 3621 independent reflections |
| Radiation source: fine-focus sealed tube | 3543 reflections with I > 2σ(I) |
| graphite | Rint = 0.032 |
| φ and ω scans | θmax = 70.2°, θmin = 2.4° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 2004) | h = −23→23 |
| Tmin = 0.622, Tmax = 0.804 | k = −10→12 |
| 31213 measured reflections | l = −12→12 |