| Bruker SMART APEXII CCD diffractometer | 11591 independent reflections |
| Radiation source: fine-focus sealed tube | 9231 reflections with I > 2σ(I) |
| graphite | Rint = 0.036 |
| φ and ω scans | θmax = 34.0°, θmin = 1.7° |
| Absorption correction: multi-scan (SADABS; Bruker, 2009) | h = −13→16 |
| Tmin = 0.943, Tmax = 0.975 | k = −18→18 |
| 39492 measured reflections | l = −19→19 |