| Rigaku R-AXIS RAPID II diffractometer | 3681 reflections with I > 2σ(I) |
| Detector resolution: 10.00 pixels mm-1 | Rint = 0.053 |
| ω scans | θmax = 29.9°, θmin = 3.1° |
| Absorption correction: numerical (NUMABS; Higashi, 1999) | h = −42→43 |
| Tmin = 0.925, Tmax = 0.983 | k = −4→5 |
| 17044 measured reflections | l = −17→17 |
| 4166 independent reflections |
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