Table 1. Data-collection statistics.
Values in parentheses are for the last shell.
| Crystals | WT (FBP, NAD+) | H171C (NAD+) | H171C (apo) |
|---|---|---|---|
| Space group | P3 | P3 | P3 |
| Unit-cell parameters | |||
| a (Å) | 171.04 | 133.43 | 133.41 |
| b (Å) | 171.04 | 133.43 | 133.41 |
| c (Å) | 96.27 | 99.09 | 99.34 |
| Data collection | |||
| Detector | MAR CCD 300 | MAR CCD 300 | MAR CCD 300 |
| Wavelength (Å) | 0.9793 | 0.9793 | 0.9793 |
| Resolution (Å) | 50.0–2.38 (2.47–2.38) | 50.0–2.49 (2.59–2.49) | 50.0–2.20 (2.28–2.20) |
| Multiplicity | 5.8 (2.7) | 5.0 (3.4) | 5.4 (4.5) |
| 〈I/σ(I)〉 | 15.9 (1.5) | 14.4 (3.1) | 18.4 (3.7) |
| Completeness (%) | 98.9 (89.9) | 99.9 (99.8) | 98.9 (99.8) |
| Rmerge (%) | 8.6 (61.0) | 9.5 (40.4) | 6.8 (39.9) |