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. 2011 Dec 21;68(Pt 1):m76. doi: 10.1107/S1600536811053785
Oxford Diffraction Gemini R Ultra diffractometer 5059 independent reflections
Radiation source: fine-focus sealed tube 3914 reflections with I > 2σ(I)
graphite Rint = 0.052
ω scans θmax = 25.4°, θmin = 3.2°
Absorption correction: multi-scan SADABS (Bruker, 2002) h = −14→11
Tmin = 0.780, Tmax = 0.910 k = −17→22
12726 measured reflections l = −15→13