Oxford Diffraction Gemini R Ultra diffractometer | 5059 independent reflections |
Radiation source: fine-focus sealed tube | 3914 reflections with I > 2σ(I) |
graphite | Rint = 0.052 |
ω scans | θmax = 25.4°, θmin = 3.2° |
Absorption correction: multi-scan SADABS (Bruker, 2002) | h = −14→11 |
Tmin = 0.780, Tmax = 0.910 | k = −17→22 |
12726 measured reflections | l = −15→13 |