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. Author manuscript; available in PMC: 2013 Jan 2.
Published in final edited form as: Inorg Chem. 2011 Dec 16;51(1):629–639. doi: 10.1021/ic202150b

Table 1.

Reaction conditions to control the degree of iodination by Strategy 1.

Reactions (Scheme 1) % in Reaction Mixturesa
Decomp. Prods. 3 (recov.) 4 N5-I2 N5-I3 5
c ~10 ~45 ~40 ~5 0 0
d ~35 0 0 0 ~10 ~55
e 100 0 0 0 0 0
a

Estimations based on TLC- and 1H-NMR analyses of reaction mixtures.