TABLE 3.

H5-H2 and H5-H4 NOE magnitudes (%) of iduronic acid residues of OCTA-2 and OCTA-4, in their free state, measured at 35 °C in phosphate buffer 10 mm, pH 7.4, and 0.5 m NaCl at three mixing time values

	Mixing	OCTA-2	OCTA-4
	ms
H5-H2 I	100	1.0	1.5
	200	2.5	1.7
	300	3.6	3.4
H5-H4 I	100	3.0	2.8
	200	5.4	5.2
	300	8.4	7.6
H5-H2 I″	100	0
	200	0
	300	0
H5-H4 I″	100	1.8
	200	2.6
	300	4.3