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. Author manuscript; available in PMC: 2013 Jan 1.
Published in final edited form as: J Magn Reson. 2011 Dec 2;214(1):258–262. doi: 10.1016/j.jmr.2011.11.015

Figure 2.

Figure 2

Apparatus for filling NMR tubes at low pressure with parahydrogen gas. V1 through V5 correspond to manual butterfly valves: V1 is an aluminum tank valve, V2 is used to normalize the apparatus to atmospheric pressure, V3 is a valve built into the cap of a low-pressure NMR tube, V4 allows evacuation of the assembly, and V5 is a relief valve for preventing inadvertent explosion of the glass components.