Table 1. Crystal characteristics and experimental set-up for the samples used in this work.
Crystal | Unit cell (Å) | Space group | Crystal size (µm) | Energy (keV) | Flux (photons s−1) | Dose rate (MGy s−1) | Total dose (MGy) | Resolution limit (Å) |
---|---|---|---|---|---|---|---|---|
Thermolysin | a = b = 93.16, c = 129.31 | P6122 | 300 × 50 × 50 | 12.76 | 6.2 × 1011 | 0.15 | ∼10 | 2.0 |
Trypsin | a = 61.87, b = 63.66, c = 68.68 | P212121 | 900 × 100 × 100 | 12.76 | 9.9 × 1011 | 0.24 | ∼10 | 2.0 |
A-DNA | a = b = 32.65, c = 77.76 | P6122 | 400 × 200 × 200 | 7.70 | 2 × 1011 | 0.14 | ∼10 | 2.0 |
FAE 1 | a = 65.4, b = 108.5, c = 113.6 | P212121 | 400 × 40 × 40 | 12.64 | 8.0 × 1011 | 0.20 | ∼10 | 2.0 |
FAE 2 | a = 65.4, b = 108.5, c = 113.6 | P212121 | 400 × 40 × 40 | 12.64 | 1.0 × 1012 | 0.24 | ∼10 to 12 | 2.0 |
RecR | a = 71.52, b = 71.95, c = 174.05 | I222 | 20 × 20 × 20 | 12.75 | 7.6 × 1011 | 0.17 | ∼15 | 3.0 |
GPCR | a = 89.18, b = 60.98, c = 101.01 | P2, β = 109.4° | 50 × 40 × 10 | 12.72 | 4.3 × 1011 | 0.10 | ∼46 | 4.2 |