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. Author manuscript; available in PMC: 2012 Feb 3.
Published in final edited form as: J Org Chem. 2008 Oct 21;73(22):8785–8790. doi: 10.1021/jo801578f

Table 3.

Application of DCT monomer 3 in a Couple-ROMP-Filter protocol

graphic file with name nihms91109t3.jpg
Entry R1CO2H R2NH2 Yield (%)c Purity (%)b
1 BnCO2H BnNH2 95 >95
2 C9H19CO2H BnNH2 93 >95
3 p-TolCO2H iPrNH2 92 >95
4 P-TolCO2H C5H8NH 93 >95
5 4-OMe-3-MeBnCO2H C5H8NH 96 >95
a

All reactions were carried out on 0.164 mmol scale, with addition of 2.0 equivalents of 3 unless stated otherwise.

b

Purity by GC and confirmed by 1H NMR.

c

Yields were calculated from pure products after purification via elution through a silica SPE.