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. 2010 Apr 7;10(4):3363–3372. doi: 10.3390/s100403363

Table 1.

Fabrication of process parameters.

STEP RECIPE
(1) Steel foil: stainless steel foil substrate (SS-304 40 μm thick)
H2SO4 + H2O2 (cleaning 10 mins)
(2) AlN sputtering:
Ar (8SCCM), N2 (2SCCM), pressure (0.32 Pa), substrate temperature (120 °C), power (170 W)
(3) Cr / Au evaporating:
substrate temperature (100 °C), background pressure (7 × 10−7Torr), Cr thickness (200 Å), Au thickness (2,000 Å)
(4) Lithography:
spin-coated photoresist→ step1:500 rpm, 5s; step2:3,000 rpm, 30 s. soft bake→ 90 °C, 120 s. exposure→ 5 mW/cm2. development→ MF319:DI water = 1:1, hard bake→ 90 °C, 300 s
(5) Au / Cr etching:
Au etching (KI + I2,7 mins), Cr etching (Cr-7, 3 mins)
(6) PI coating:
spin-coated polyimide→ step1:500 rpm, 5s; step2:3,000 rpm, 30s. soft bake→ 90 °C, 120 s. exposure→ 5 mW/cm2. development→ (HTR D-2):(RER 600) = 1:2, hard bake→ 90 °C, 300 s
(7) PR coating:
spin-coated photoresist→ step1:500 rpm, 5 s; step2:3,000 rpm, 30 s. soft bake→ 90 °C, 120 s.
(8) Define protection layer:
exposure→ 5m W/cm2. development→ MF319:DI water = 1:1, hard bake→ 90 °C, 300 s
(9) Steel foil etching:
aqua regia (50 °C)