Table 1. Data-collection statistics.
NtCPIP1-Δ(1:127) | NtCPIP1-wt | |
---|---|---|
Beamline | BESSY-MX BL14.1 | |
Detector | Rayonics MX-225 3 × 3 CCD detector | |
Temperature (K) | 100 | |
Space group | P21212 | C222 |
Unit-cell parameters (Å, °) | a = 65.6, b = 141.5, c = 50.9, α = β = γ = 90 | a = 136.8, b = 260.8, c = 378.2, α = β = γ = 90 |
Wavelength (Å) | 0.9180 | 0.9180 |
Resolution range (Å) | 35.0–2.38 (2.44–2.38) | 20.0–8.00 (8.21–8.00) |
Unique reflections | 19599 (1409) | 6569 (538) |
Multiplicity | 4.0 (3.8) | 3.8 (3.8) |
Completeness (%) | 99.6 (98.1) | 87.2 (95.6) |
Mean I/σ(I) | 15.8 (2.5) | 8.7 (1.6) |
Rmeas† (%) | 7.6 (61.1) | 16.8 (85.3) |
Rmrgd-F‡ (%) | 13.9 (83.2) | 26.6 (110.2) |