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. Author manuscript; available in PMC: 2012 Apr 25.
Published in final edited form as: J Org Chem. 2010 Oct 25;75(22):7682–7690. doi: 10.1021/jo101498b

Table 3.

Thermal Phase Behavior Characterization - 1:1 Mixtures of D1-10:N1

Derivative graphic file with name nihms248107t1.jpg
D1N1 D1 EVAPORATED
D2N1 D2 EVAPORATED
D3N1 D3 EVAPORATED
D4N1 D4 EVAPORATED
D5N1 Iso 188 [−13] graphic file with name nihms248107t2.jpg 72 [−31] graphic file with name nihms248107t2.jpg 55 [−87] Cr
D6N1 Iso 182 [−4] graphic file with name nihms248107t2.jpg 71a [−82] Cr
D7N1 Iso 176 [−13] graphic file with name nihms248107t2.jpg 71 [−19] graphic file with name nihms248107t2.jpg 53 [−43] Cr
D8N1 Iso 182 [−8] graphic file with name nihms248107t2.jpg 74a [−93] Cr
D9N1 D9 EVAPORATED
D10N1 D10 EVAPORATED

Temperatures (°C) and enthalpies (KJ/mol) in brackets for phase transitions determined by DSC upon cooling 2°C/min. Tc is a transition upon cooling. Iso = isotropic and Cr = final crystalline state.

(a)

Transition is composed of multiple peaks.