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. Author manuscript; available in PMC: 2012 Apr 25.
Published in final edited form as: J Org Chem. 2010 Oct 25;75(22):7682–7690. doi: 10.1021/jo101498b

Table 4.

Thermal Phase Behavior Characterization - 1:1 Mixtures of D1-10:N2

Derivative graphic file with name nihms248107t1.jpg
D1N2 D1 EVAPORATED
D2N2 Iso 137 [−10] graphic file with name nihms248107t2.jpg 86 [−28] graphic file with name nihms248107t2.jpg 81a [−22] Cr
D3N2 Iso 139 [−8] graphic file with name nihms248107t2.jpg 64 [−47] Cr
D4N2 Iso 148 [−7] graphic file with name nihms248107t2.jpg 78 [−62] Cr
D5N2 Iso 138 [−9] graphic file with name nihms248107t2.jpg 60 [−55] Cr
D6N2 Iso 140 [−8] graphic file with name nihms248107t2.jpg 76 [−74] Cr
D7N2 Iso 146 [−7] graphic file with name nihms248107t2.jpg 68 [−68] Cr
D8N2 Iso 141 [−6] graphic file with name nihms248107t2.jpg 78 [−92] Cr
D9N2 D9 EVAPORATED
D10N2 Iso 144 [−10] graphic file with name nihms248107t2.jpg 41 [−0.6] Cr

Temperatures (°C) and enthalpies (KJ/mol) in brackets for phase transitions determined by DSC upon cooling 2°C/min. Tc is a transition upon cooling. Iso = isotropic and Cr = final crystalline state.

(a)

Transition is composed of multiple peaks.