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. Author manuscript; available in PMC: 2012 Apr 25.
Published in final edited form as: J Org Chem. 2010 Oct 25;75(22):7682–7690. doi: 10.1021/jo101498b

Table 6.

12Thermal Phase Behavior Characterization - 1:1 Mixtures of D1-10:N4

Derivative graphic file with name nihms248107t1.jpg
D1N4 D1 EVAPORATED
D2N4 Iso 116 [−4] graphic file with name nihms248107t2.jpg 103 [−17] graphic file with name nihms248107t2.jpg 83 [−9] Cr
D3N4 Iso 121 [−7] graphic file with name nihms248107t2.jpg 99 [−18] graphic file with name nihms248107t2.jpg 65 [−22] Cr
D4N4 Iso 129 [−5] graphic file with name nihms248107t2.jpg 122 [−41] graphic file with name nihms248107t2.jpg 72 [−5] Cr
D5N4 Iso 133 [−11] graphic file with name nihms248107t2.jpg 124 [−35] Cr
D6N4 Iso 123a [−5] graphic file with name nihms248107t2.jpg 121a [−40] Cr
D7N4 Iso 124 [−7] graphic file with name nihms248107t2.jpg 112 [−35] graphic file with name nihms248107t2.jpg 61 [−18] Cr
D8N4 Iso 115 [−7] graphic file with name nihms248107t2.jpg 99 [−20] graphic file with name nihms248107t2.jpg 76 [−49] Cr
D9N4 Iso 115 [−10] graphic file with name nihms248107t2.jpg 80 [−42] Cr
D10N4 Iso 122 [−11] graphic file with name nihms248107t2.jpg 20 [−15] Cr

Temperatures (°C) and enthalpies (KJ/mol) in brackets for phase transitions determined by DSC upon cooling 2°C/min. Tc is a transition upon cooling. Iso = isotropic and Cr = final crystalline state.

(a)

Transition is composed of multiple peaks.