Skip to main content
. Author manuscript; available in PMC: 2012 Apr 25.
Published in final edited form as: J Org Chem. 2010 Oct 25;75(22):7682–7690. doi: 10.1021/jo101498b

Table 7.

Thermal Phase Behavior Characterization - 1:1 Mixtures of D1-10:N5

Derivative graphic file with name nihms248107t1.jpg
D1N5 Iso 95 [−0.7] graphic file with name nihms248107t2.jpg 84 [−5] Cr
D2N5 Iso 98 [−42] graphic file with name nihms248107t2.jpg 89 [−3] graphic file with name nihms248107t2.jpg 63 [−11] Cr
D3N5 Iso 95 [−37] graphic file with name nihms248107t2.jpg 61 [−10] Cr
D4N5 Iso 111 [−52] graphic file with name nihms248107t2.jpg 77 [−3] Cr
D5N5 Iso 110 [−54] graphic file with name nihms248107t2.jpg 50 [−11] Cr
D6N5 Iso 110 [−59] graphic file with name nihms248107t2.jpg 73 [−3] Cr
D7N5 Iso 106 [−58] graphic file with name nihms248107t2.jpg 55 [−3] Cr
D8N5 Iso 94 [−55] graphic file with name nihms248107t2.jpg 74 [−16] Cr
D9N5 Iso 106 [−50] graphic file with name nihms248107t2.jpg 81 [−3] Cr
D10 N5 Iso --- ---

Temperatures (°C) and enthalpies (KJ/mol) in brackets for phase transitions determined by DSC upon cooling 2°C/min. Tc is a transition upon cooling. Iso = isotropic and Cr = final crystalline state. Dashes indicate no observed exothermic transitions.