Bruker APEXII CCD diffractometer | 3083 independent reflections |
Radiation source: fine-focus sealed tube | 2207 reflections with I > 2σ(I) |
graphite | Rint = 0.022 |
φ and ω scans | θmax = 25.5°, θmin = 2.4° |
Absorption correction: multi-scan (SADABS; Bruker, 2004) | h = −8→8 |
Tmin = 0.936, Tmax = 0.948 | k = −9→9 |
5579 measured reflections | l = −20→17 |