| Stoe IPDS diffractometer | 6486 independent reflections |
| Radiation source: fine-focus sealed tube | 3306 reflections with I > 2σ(I) |
| graphite | Rint = 0.068 |
| Detector resolution: 6.7 pixels mm-1 | θmax = 25.0°, θmin = 2.1° |
| φ–scans | h = −10→10 |
| Absorption correction: multi-scan (Blessing, 1995) | k = −48→48 |
| Tmin = 0.972, Tmax = 1.000 | l = −12→12 |
| 28928 measured reflections |
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