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. 2012 Jan 18;68(Pt 2):o446. doi: 10.1107/S1600536811054985
Rigaku Saturn724 CCD diffractometer 3904 independent reflections
Radiation source: rotating anode 3461 reflections with I > 2σ(I)
multilayer Rint = 0.070
Detector resolution: 14.22 pixels mm-1 θmax = 27.9°, θmin = 1.9°
ω and φ scans h = −14→14
Absorption correction: multi-scan (CrystalClear; Rigaku/MSC, 2002) k = −14→13
Tmin = 0.959, Tmax = 0.979 l = −17→17
16805 measured reflections