| Agilent Xcalibur Eos diffractometer | 1446 independent reflections |
| Radiation source: fine-focus sealed tube | 1189 reflections with I > 2σ(I) |
| graphite | Rint = 0.026 |
| Detector resolution: 16.1593 pixels mm-1 | θmax = 26.0°, θmin = 3.0° |
| ω scans | h = −5→6 |
| Absorption correction: multi-scan (CrysAlis PRO; Agilent, 2011) | k = −8→7 |
| Tmin = 0.914, Tmax = 1.000 | l = −12→8 |
| 2575 measured reflections |
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