Bruker APEXII CCD diffractometer | 2075 reflections with I > 2σ(I) |
Radiation source: sealed tube | Rint = 0.030 |
graphite | θmax = 28.3°, θmin = 3.4° |
φ and ω scans | h = −14→14 |
12714 measured reflections | k = −6→8 |
3365 independent reflections | l = −26→26 |