| Bruker APEXII CCD diffractometer | 2075 reflections with I > 2σ(I) |
| Radiation source: sealed tube | Rint = 0.030 |
| graphite | θmax = 28.3°, θmin = 3.4° |
| φ and ω scans | h = −14→14 |
| 12714 measured reflections | k = −6→8 |
| 3365 independent reflections | l = −26→26 |
| Bruker APEXII CCD diffractometer | 2075 reflections with I > 2σ(I) |
| Radiation source: sealed tube | Rint = 0.030 |
| graphite | θmax = 28.3°, θmin = 3.4° |
| φ and ω scans | h = −14→14 |
| 12714 measured reflections | k = −6→8 |
| 3365 independent reflections | l = −26→26 |