| Bruker APEXII CCD diffractometer | 1961 independent reflections |
| Radiation source: fine-focus sealed tube | 1248 reflections with I > 2σ(I) |
| graphite | Rint = 0.024 |
| φ and ω scans | θmax = 27.1°, θmin = 3.2° |
| Absorption correction: multi-scan (SADABS; Bruker, 2007) | h = −10→10 |
| Tmin = 0.671, Tmax = 0.746 | k = −18→17 |
| 8725 measured reflections | l = −20→15 |