Rigaku Saturn CCD area-detector diffractometer	9251 independent reflections
Radiation source: rotating anode	6476 reflections with I > 2σ(I)
multilayer	Rint = 0.037
Detector resolution: 14.22 pixels mm-1	θmax = 27.9°, θmin = 2.0°
φ and ω scans	h = −12→12
Absorption correction: multi-scan (CrystalClear; Rigaku/MSC, 2005)	k = −12→12
Tmin = 0.985, Tmax = 0.993	l = −27→27
25242 measured reflections