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. 2012 Jan 31;68(Pt 2):o552. doi: 10.1107/S1600536812002450
Cl1—C30 1.741 (3) C21—H21 0.9300
Cl1'—C30' 1.746 (4) C23—H23 0.9300
O40—C39 1.312 (3) C28—H28 0.9300
O40—C41 1.467 (6) C29—H29 0.9300
O43—C39 1.191 (4) C31—H31 0.9300
O44—C6 1.220 (3) C32—H32 0.9300
O45—C4 1.202 (3) C34—H34 0.9300
O40'—C41' 1.478 (6) C35—H35 0.9300
O40'—C39' 1.308 (5) C36—H36 0.9300
O43'—C39' 1.199 (4) C37—H37 0.9300
O44'—C6' 1.208 (3) C38—H38 0.9300
O45'—C4' 1.193 (3) C41—H41A 0.9700
N2—C1 1.466 (3) C41—H41B 0.9700
N2—C3 1.488 (3) C42—H42E 0.9600
N2—C9 1.442 (4) C42—H42F 0.9600
N5—C16 1.432 (4) C42—H42D 0.9600
N5—C6 1.386 (3) C1'—C7' 1.534 (3)
N5—C4 1.395 (3) C1'—C39' 1.517 (5)
N24—N25 1.358 (3) C3'—C8' 1.564 (4)
N24—C23 1.349 (3) C3'—C22' 1.499 (4)
N24—C33 1.430 (4) C4'—C8' 1.507 (4)
N25—C26 1.338 (3) C6'—C7' 1.505 (3)
N2'—C1' 1.457 (4) C7'—C8' 1.524 (4)
N2'—C3' 1.472 (3) C9'—C10' 1.513 (4)
N2'—C9' 1.463 (4) C10'—C11' 1.373 (5)
N5'—C16' 1.440 (3) C10'—C15' 1.382 (5)
N5'—C4' 1.393 (3) C11'—C12' 1.369 (5)
N5'—C6' 1.390 (4) C12'—C13' 1.365 (6)
N24'—C23' 1.358 (4) C13'—C14' 1.366 (7)
N24'—C33' 1.424 (4) C14'—C15' 1.385 (5)
N24'—N25' 1.362 (3) C16'—C17' 1.372 (4)
N25'—C26' 1.328 (4) C16'—C21' 1.384 (5)
C1—C7 1.506 (4) C17'—C18' 1.383 (5)
C1—C39 1.534 (5) C18'—C19' 1.382 (7)
C3—C8 1.553 (3) C19'—C20' 1.364 (6)
C3—C22 1.509 (4) C20'—C21' 1.377 (5)
C4—C8 1.511 (4) C22'—C23' 1.368 (4)
C6—C7 1.505 (4) C22'—C26' 1.406 (4)
C7—C8 1.524 (3) C26'—C27' 1.487 (4)
C9—C10 1.517 (4) C27'—C28' 1.381 (4)
C10—C15 1.379 (6) C27'—C32' 1.374 (4)
C10—C11 1.382 (5) C28'—C29' 1.377 (5)
C11—C12 1.393 (5) C29'—C30' 1.371 (5)
C12—C13 1.341 (7) C30'—C31' 1.376 (5)
C13—C14 1.379 (6) C31'—C32' 1.389 (5)
C14—C15 1.397 (5) C33'—C34' 1.363 (5)
C16—C17 1.373 (5) C33'—C38' 1.373 (6)
C16—C21 1.378 (5) C34'—C35' 1.396 (8)
C17—C18 1.393 (6) C35'—C36' 1.354 (7)
C18—C19 1.347 (6) C36'—C37' 1.348 (6)
C19—C20 1.404 (6) C37'—C38' 1.367 (8)
C20—C21 1.382 (6) C41'—C42' 1.484 (11)
C22—C26 1.425 (3) C1'—H1' 0.9800
C22—C23 1.353 (4) C3'—H3' 0.9800
C26—C27 1.473 (4) C7'—H7' 0.9800
C27—C32 1.388 (5) C8'—H8' 0.9800
C27—C28 1.375 (3) C9'—H9'1 0.9700
C28—C29 1.376 (4) C9'—H9'2 0.9700
C29—C30 1.341 (5) C11'—H11' 0.9300
C30—C31 1.375 (4) C12'—H12' 0.9300
C31—C32 1.373 (5) C13'—H13' 0.9300
C33—C38 1.368 (4) C14'—H14' 0.9300
C33—C34 1.362 (5) C15'—H15' 0.9300
C34—C35 1.381 (6) C17'—H17' 0.9300
C35—C36 1.361 (6) C18'—H18' 0.9300
C36—C37 1.350 (5) C19'—H19' 0.9300
C37—C38 1.384 (6) C20'—H20' 0.9300
C41—C42 1.443 (7) C21'—H21' 0.9300
C1—H1 0.9800 C23'—H23' 0.9300
C3—H3 0.9800 C28'—H28' 0.9300
C7—H7 0.9800 C29'—H29' 0.9300
C8—H8 0.9800 C31'—H31' 0.9300
C9—H91 0.9700 C32'—H32' 0.9300
C9—H92 0.9700 C34'—H34' 0.9300
C11—H11 0.9300 C35'—H35' 0.9300
C12—H12 0.9300 C36'—H36' 0.9300
C13—H13 0.9300 C37'—H37' 0.9300
C14—H14 0.9300 C38'—H38' 0.9300
C15—H15 0.9300 C41'—H41C 0.9700
C17—H17 0.9300 C41'—H41D 0.9700
C18—H18 0.9300 C42'—H42A 0.9600
C19—H19 0.9300 C42'—H42B 0.9600
C20—H20 0.9300 C42'—H42C 0.9600
C39—O40—C41 116.5 (3) O40—C41—H41A 110.00
C39'—O40'—C41' 117.1 (3) O40—C41—H41B 110.00
C1—N2—C9 115.9 (2) C42—C41—H41A 110.00
C3—N2—C9 114.8 (2) C42—C41—H41B 110.00
C1—N2—C3 107.05 (18) H41A—C41—H41B 108.00
C4—N5—C6 112.4 (2) C41—C42—H42F 110.00
C4—N5—C16 122.9 (2) H42E—C42—H42F 109.00
C6—N5—C16 124.6 (2) H42D—C42—H42E 109.00
N25—N24—C23 110.7 (2) H42D—C42—H42F 110.00
N25—N24—C33 119.8 (2) C41—C42—H42D 110.00
C23—N24—C33 129.5 (2) C41—C42—H42E 109.00
N24—N25—C26 105.6 (2) N2'—C1'—C7' 101.5 (2)
C1'—N2'—C9' 116.1 (2) N2'—C1'—C39' 116.0 (2)
C3'—N2'—C9' 114.7 (2) C7'—C1'—C39' 110.1 (2)
C1'—N2'—C3' 107.4 (2) N2'—C3'—C8' 103.9 (2)
C6'—N5'—C16' 124.6 (2) N2'—C3'—C22' 110.9 (2)
C4'—N5'—C6' 112.5 (2) C8'—C3'—C22' 113.1 (2)
C4'—N5'—C16' 122.7 (2) O45'—C4'—N5' 125.0 (2)
C23'—N24'—C33' 128.2 (2) O45'—C4'—C8' 127.9 (2)
N25'—N24'—C23' 111.4 (2) N5'—C4'—C8' 107.1 (2)
N25'—N24'—C33' 120.3 (2) O44'—C6'—N5' 124.8 (2)
N24'—N25'—C26' 104.7 (2) O44'—C6'—C7' 126.8 (3)
N2—C1—C39 113.5 (2) N5'—C6'—C7' 108.4 (2)
C7—C1—C39 110.6 (2) C1'—C7'—C6' 112.0 (2)
N2—C1—C7 101.6 (2) C1'—C7'—C8' 105.9 (2)
N2—C3—C8 102.79 (18) C6'—C7'—C8' 104.3 (2)
N2—C3—C22 109.7 (2) C3'—C8'—C4' 113.5 (2)
C8—C3—C22 116.5 (2) C3'—C8'—C7' 104.4 (2)
O45—C4—N5 124.9 (3) C4'—C8'—C7' 104.93 (19)
O45—C4—C8 127.3 (3) N2'—C9'—C10' 111.9 (3)
N5—C4—C8 107.8 (2) C9'—C10'—C11' 121.1 (3)
O44—C6—N5 124.7 (3) C9'—C10'—C15' 120.6 (3)
O44—C6—C7 126.7 (2) C11'—C10'—C15' 118.3 (3)
N5—C6—C7 108.6 (2) C10'—C11'—C12' 121.3 (3)
C6—C7—C8 104.8 (2) C11'—C12'—C13' 120.1 (4)
C1—C7—C8 106.6 (2) C12'—C13'—C14' 119.8 (4)
C1—C7—C6 110.3 (2) C13'—C14'—C15' 120.2 (4)
C3—C8—C4 112.1 (2) C10'—C15'—C14' 120.2 (4)
C3—C8—C7 105.01 (19) N5'—C16'—C17' 120.8 (3)
C4—C8—C7 104.6 (2) N5'—C16'—C21' 118.9 (2)
N2—C9—C10 113.8 (3) C17'—C16'—C21' 120.3 (3)
C9—C10—C15 122.4 (3) C16'—C17'—C18' 119.9 (4)
C11—C10—C15 117.3 (3) C17'—C18'—C19' 119.8 (3)
C9—C10—C11 120.3 (3) C18'—C19'—C20' 119.8 (4)
C10—C11—C12 121.0 (4) C19'—C20'—C21' 121.0 (4)
C11—C12—C13 121.5 (4) C16'—C21'—C20' 119.2 (3)
C12—C13—C14 118.6 (4) C3'—C22'—C23' 127.5 (2)
C13—C14—C15 120.7 (4) C3'—C22'—C26' 127.0 (2)
C10—C15—C14 120.9 (3) C23'—C22'—C26' 104.6 (2)
N5—C16—C17 119.3 (3) N24'—C23'—C22' 107.5 (2)
N5—C16—C21 120.1 (3) N25'—C26'—C22' 111.9 (2)
C17—C16—C21 120.6 (3) N25'—C26'—C27' 118.9 (2)
C16—C17—C18 119.6 (3) C22'—C26'—C27' 129.1 (3)
C17—C18—C19 120.7 (4) C26'—C27'—C28' 118.9 (2)
C18—C19—C20 119.7 (4) C26'—C27'—C32' 122.4 (3)
C19—C20—C21 119.9 (4) C28'—C27'—C32' 118.7 (3)
C16—C21—C20 119.5 (3) C27'—C28'—C29' 121.9 (3)
C3—C22—C26 130.1 (2) C28'—C29'—C30' 118.0 (3)
C23—C22—C26 104.4 (2) Cl1'—C30'—C29' 118.1 (3)
C3—C22—C23 125.5 (2) Cl1'—C30'—C31' 120.0 (3)
N24—C23—C22 109.0 (2) C29'—C30'—C31' 121.9 (3)
N25—C26—C27 117.4 (2) C30'—C31'—C32' 118.7 (3)
C22—C26—C27 132.2 (2) C27'—C32'—C31' 120.7 (3)
N25—C26—C22 110.3 (2) N24'—C33'—C34' 120.6 (3)
C28—C27—C32 115.4 (3) N24'—C33'—C38' 120.4 (3)
C26—C27—C28 119.8 (3) C34'—C33'—C38' 119.0 (4)
C26—C27—C32 124.7 (2) C33'—C34'—C35' 119.5 (4)
C27—C28—C29 122.7 (3) C34'—C35'—C36' 120.9 (4)
C28—C29—C30 120.2 (2) C35'—C36'—C37' 118.7 (5)
Cl1—C30—C31 119.8 (3) C36'—C37'—C38' 121.7 (5)
C29—C30—C31 119.7 (3) C33'—C38'—C37' 120.0 (4)
Cl1—C30—C29 120.45 (19) O40'—C39'—O43' 123.9 (4)
C30—C31—C32 119.4 (4) O40'—C39'—C1' 110.7 (3)
C27—C32—C31 122.4 (3) O43'—C39'—C1' 125.4 (4)
N24—C33—C34 120.8 (3) O40'—C41'—C42' 104.3 (5)
N24—C33—C38 120.0 (3) N2'—C1'—H1' 110.00
C34—C33—C38 119.2 (3) C7'—C1'—H1' 110.00
C33—C34—C35 120.5 (4) C39'—C1'—H1' 110.00
C34—C35—C36 120.4 (4) N2'—C3'—H3' 110.00
C35—C36—C37 119.0 (4) C8'—C3'—H3' 110.00
C36—C37—C38 121.3 (4) C22'—C3'—H3' 110.00
C33—C38—C37 119.6 (3) C1'—C7'—H7' 111.00
O40—C39—O43 124.6 (4) C6'—C7'—H7' 111.00
O40—C39—C1 111.3 (3) C8'—C7'—H7' 111.00
O43—C39—C1 124.1 (3) C3'—C8'—H8' 111.00
O40—C41—C42 108.9 (4) C4'—C8'—H8' 111.00
C7—C1—H1 110.00 C7'—C8'—H8' 111.00
C39—C1—H1 110.00 N2'—C9'—H9'1 109.00
N2—C1—H1 110.00 N2'—C9'—H9'2 109.00
N2—C3—H3 109.00 C10'—C9'—H9'1 109.00
C8—C3—H3 109.00 C10'—C9'—H9'2 109.00
C22—C3—H3 109.00 H9'1—C9'—H9'2 108.00
C6—C7—H7 112.00 C10'—C11'—H11' 119.00
C8—C7—H7 112.00 C12'—C11'—H11' 119.00
C1—C7—H7 112.00 C11'—C12'—H12' 120.00
C4—C8—H8 112.00 C13'—C12'—H12' 120.00
C7—C8—H8 112.00 C12'—C13'—H13' 120.00
C3—C8—H8 112.00 C14'—C13'—H13' 120.00
H91—C9—H92 108.00 C13'—C14'—H14' 120.00
C10—C9—H92 109.00 C15'—C14'—H14' 120.00
C10—C9—H91 109.00 C10'—C15'—H15' 120.00
N2—C9—H91 109.00 C14'—C15'—H15' 120.00
N2—C9—H92 109.00 C16'—C17'—H17' 120.00
C12—C11—H11 119.00 C18'—C17'—H17' 120.00
C10—C11—H11 120.00 C17'—C18'—H18' 120.00
C13—C12—H12 119.00 C19'—C18'—H18' 120.00
C11—C12—H12 119.00 C18'—C19'—H19' 120.00
C12—C13—H13 121.00 C20'—C19'—H19' 120.00
C14—C13—H13 121.00 C19'—C20'—H20' 119.00
C15—C14—H14 120.00 C21'—C20'—H20' 120.00
C13—C14—H14 120.00 C16'—C21'—H21' 120.00
C10—C15—H15 120.00 C20'—C21'—H21' 120.00
C14—C15—H15 120.00 N24'—C23'—H23' 126.00
C16—C17—H17 120.00 C22'—C23'—H23' 126.00
C18—C17—H17 120.00 C27'—C28'—H28' 119.00
C17—C18—H18 120.00 C29'—C28'—H28' 119.00
C19—C18—H18 120.00 C28'—C29'—H29' 121.00
C20—C19—H19 120.00 C30'—C29'—H29' 121.00
C18—C19—H19 120.00 C30'—C31'—H31' 121.00
C21—C20—H20 120.00 C32'—C31'—H31' 121.00
C19—C20—H20 120.00 C27'—C32'—H32' 120.00
C16—C21—H21 120.00 C31'—C32'—H32' 120.00
C20—C21—H21 120.00 C33'—C34'—H34' 120.00
C22—C23—H23 126.00 C35'—C34'—H34' 120.00
N24—C23—H23 125.00 C34'—C35'—H35' 120.00
C29—C28—H28 119.00 C36'—C35'—H35' 120.00
C27—C28—H28 119.00 C35'—C36'—H36' 121.00
C28—C29—H29 120.00 C37'—C36'—H36' 121.00
C30—C29—H29 120.00 C36'—C37'—H37' 119.00
C30—C31—H31 120.00 C38'—C37'—H37' 119.00
C32—C31—H31 120.00 C33'—C38'—H38' 120.00
C31—C32—H32 119.00 C37'—C38'—H38' 120.00
C27—C32—H32 119.00 O40'—C41'—H41C 111.00
C33—C34—H34 120.00 O40'—C41'—H41D 111.00
C35—C34—H34 120.00 C42'—C41'—H41C 111.00
C36—C35—H35 120.00 C42'—C41'—H41D 111.00
C34—C35—H35 120.00 H41C—C41'—H41D 109.00
C35—C36—H36 121.00 C41'—C42'—H42A 109.00
C37—C36—H36 120.00 C41'—C42'—H42B 109.00
C36—C37—H37 119.00 C41'—C42'—H42C 109.00
C38—C37—H37 119.00 H42A—C42'—H42B 110.00
C37—C38—H38 120.00 H42A—C42'—H42C 109.00
C33—C38—H38 120.00 H42B—C42'—H42C 110.00
C41—O40—C39—O43 5.6 (5) C21—C16—C17—C18 1.4 (5)
C41—O40—C39—C1 −174.1 (3) N5—C16—C21—C20 176.7 (3)
C39—O40—C41—C42 −170.8 (3) C17—C16—C21—C20 −1.3 (5)
C39'—O40'—C41'—C42' 161.3 (4) C16—C17—C18—C19 −0.3 (6)
C41'—O40'—C39'—O43' −4.5 (5) C17—C18—C19—C20 −0.8 (6)
C41'—O40'—C39'—C1' 175.5 (3) C18—C19—C20—C21 0.9 (6)
C3—N2—C1—C39 −76.4 (3) C19—C20—C21—C16 0.1 (5)
C1—N2—C3—C8 −35.2 (3) C3—C22—C26—N25 −178.3 (2)
C9—N2—C1—C7 171.9 (2) C23—C22—C26—C27 178.4 (3)
C9—N2—C1—C39 53.2 (3) C3—C22—C26—C27 0.2 (5)
C3—N2—C1—C7 42.3 (3) C23—C22—C26—N25 0.0 (3)
C1—N2—C9—C10 74.3 (3) C26—C22—C23—N24 0.0 (3)
C3—N2—C9—C10 −160.0 (2) C3—C22—C23—N24 178.4 (2)
C9—N2—C3—C8 −165.4 (2) N25—C26—C27—C28 1.7 (4)
C9—N2—C3—C22 70.1 (3) N25—C26—C27—C32 −174.9 (3)
C1—N2—C3—C22 −159.7 (2) C22—C26—C27—C28 −176.6 (3)
C6—N5—C4—O45 −171.1 (3) C22—C26—C27—C32 6.8 (5)
C6—N5—C4—C8 9.8 (3) C32—C27—C28—C29 −2.8 (5)
C4—N5—C6—C7 −1.4 (3) C26—C27—C32—C31 −179.3 (3)
C16—N5—C6—O44 −4.1 (4) C26—C27—C28—C29 −179.7 (3)
C16—N5—C6—C7 175.9 (2) C28—C27—C32—C31 4.0 (5)
C4—N5—C16—C17 118.1 (3) C27—C28—C29—C30 −1.1 (5)
C4—N5—C16—C21 −60.0 (4) C28—C29—C30—C31 3.8 (5)
C6—N5—C16—C17 −59.0 (4) C28—C29—C30—Cl1 −176.9 (3)
C6—N5—C16—C21 123.0 (3) C29—C30—C31—C32 −2.6 (5)
C16—N5—C4—C8 −167.6 (2) Cl1—C30—C31—C32 178.1 (3)
C4—N5—C6—O44 178.6 (2) C30—C31—C32—C27 −1.4 (6)
C16—N5—C4—O45 11.5 (4) N24—C33—C34—C35 −178.1 (3)
N25—N24—C23—C22 0.0 (3) C38—C33—C34—C35 −0.4 (6)
N25—N24—C33—C34 −177.5 (3) N24—C33—C38—C37 177.6 (3)
N25—N24—C33—C38 4.8 (4) C34—C33—C38—C37 −0.2 (5)
C33—N24—C23—C22 179.1 (3) C33—C34—C35—C36 0.1 (7)
C23—N24—N25—C26 −0.1 (3) C34—C35—C36—C37 0.8 (7)
C33—N24—N25—C26 −179.2 (2) C35—C36—C37—C38 −1.4 (6)
C23—N24—C33—C38 −174.2 (3) C36—C37—C38—C33 1.2 (6)
C23—N24—C33—C34 3.5 (5) N2'—C1'—C7'—C6' −79.5 (3)
N24—N25—C26—C22 0.1 (3) N2'—C1'—C7'—C8' 33.6 (2)
N24—N25—C26—C27 −178.7 (2) C39'—C1'—C7'—C6' 157.1 (3)
C3'—N2'—C1'—C39' 77.0 (3) C39'—C1'—C7'—C8' −89.8 (3)
C9'—N2'—C1'—C7' −172.1 (2) N2'—C1'—C39'—O40' 158.6 (2)
C9'—N2'—C1'—C39' −52.9 (3) N2'—C1'—C39'—O43' −21.4 (4)
C1'—N2'—C3'—C8' 34.1 (2) C7'—C1'—C39'—O40' −87.0 (3)
C1'—N2'—C9'—C10' −51.9 (4) C7'—C1'—C39'—O43' 93.0 (4)
C3'—N2'—C9'—C10' −178.2 (3) N2'—C3'—C8'—C4' 102.3 (2)
C9'—N2'—C3'—C8' 164.7 (3) N2'—C3'—C8'—C7' −11.3 (3)
C9'—N2'—C3'—C22' −73.4 (3) C22'—C3'—C8'—C4' −18.1 (3)
C1'—N2'—C3'—C22' 155.9 (2) C22'—C3'—C8'—C7' −131.7 (2)
C3'—N2'—C1'—C7' −42.3 (2) N2'—C3'—C22'—C23' −24.9 (3)
C6'—N5'—C4'—O45' 167.6 (3) N2'—C3'—C22'—C26' 167.8 (2)
C6'—N5'—C4'—C8' −12.1 (3) C8'—C3'—C22'—C23' 91.4 (3)
C16'—N5'—C6'—C7' 176.6 (2) C8'—C3'—C22'—C26' −75.9 (3)
C4'—N5'—C16'—C17' 127.5 (3) O45'—C4'—C8'—C3' 83.4 (3)
C4'—N5'—C16'—C21' −52.7 (4) O45'—C4'—C8'—C7' −163.2 (3)
C6'—N5'—C16'—C17' −46.2 (4) N5'—C4'—C8'—C3' −96.8 (3)
C6'—N5'—C16'—C21' 133.6 (3) N5'—C4'—C8'—C7' 16.6 (3)
C16'—N5'—C4'—C8' 173.5 (2) O44'—C6'—C7'—C1' −58.5 (4)
C4'—N5'—C6'—O44' −176.9 (3) O44'—C6'—C7'—C8' −172.6 (3)
C4'—N5'—C6'—C7' 2.3 (3) N5'—C6'—C7'—C1' 122.3 (2)
C16'—N5'—C6'—O44' −2.6 (4) N5'—C6'—C7'—C8' 8.2 (3)
C16'—N5'—C4'—O45' −6.8 (4) C1'—C7'—C8'—C3' −13.5 (3)
N25'—N24'—C33'—C34' −177.6 (3) C1'—C7'—C8'—C4' −133.1 (2)
N25'—N24'—C33'—C38' 5.1 (4) C6'—C7'—C8'—C3' 104.9 (2)
C23'—N24'—N25'—C26' −0.6 (3) C6'—C7'—C8'—C4' −14.8 (3)
C33'—N24'—N25'—C26' −177.6 (2) N2'—C9'—C10'—C11' 111.5 (4)
N25'—N24'—C23'—C22' 0.4 (3) N2'—C9'—C10'—C15' −65.9 (5)
C33'—N24'—C23'—C22' 177.1 (2) C9'—C10'—C11'—C12' −178.2 (4)
C23'—N24'—C33'—C34' 5.9 (5) C15'—C10'—C11'—C12' −0.8 (6)
C23'—N24'—C33'—C38' −171.4 (3) C9'—C10'—C15'—C14' 178.0 (4)
N24'—N25'—C26'—C27' 176.4 (2) C11'—C10'—C15'—C14' 0.5 (6)
N24'—N25'—C26'—C22' 0.6 (3) C10'—C11'—C12'—C13' 0.3 (7)
N2—C1—C7—C8 −32.2 (3) C11'—C12'—C13'—C14' 0.6 (7)
C39—C1—C7—C6 −158.2 (2) C12'—C13'—C14'—C15' −0.8 (7)
C39—C1—C7—C8 88.5 (2) C13'—C14'—C15'—C10' 0.3 (6)
N2—C1—C7—C6 81.0 (2) N5'—C16'—C17'—C18' −179.5 (3)
N2—C1—C39—O40 −121.1 (2) C21'—C16'—C17'—C18' 0.7 (4)
N2—C1—C39—O43 59.2 (4) N5'—C16'—C21'—C20' 179.0 (3)
C7—C1—C39—O40 125.5 (2) C17'—C16'—C21'—C20' −1.2 (5)
C7—C1—C39—O43 −54.3 (4) C16'—C17'—C18'—C19' −0.3 (5)
N2—C3—C8—C7 13.6 (3) C17'—C18'—C19'—C20' 0.3 (6)
C22—C3—C8—C4 20.6 (3) C18'—C19'—C20'—C21' −0.7 (6)
N2—C3—C8—C4 −99.3 (2) C19'—C20'—C21'—C16' 1.2 (6)
C8—C3—C22—C23 −93.0 (3) C3'—C22'—C23'—N24' −169.6 (2)
C8—C3—C22—C26 85.0 (3) C26'—C22'—C23'—N24' 0.0 (3)
N2—C3—C22—C26 −158.9 (3) C3'—C22'—C26'—N25' 169.3 (2)
C22—C3—C8—C7 133.6 (2) C3'—C22'—C26'—C27' −6.0 (4)
N2—C3—C22—C23 23.2 (4) C23'—C22'—C26'—N25' −0.4 (3)
O45—C4—C8—C3 −79.6 (3) C23'—C22'—C26'—C27' −175.6 (2)
O45—C4—C8—C7 167.2 (3) N25'—C26'—C27'—C28' −46.2 (4)
N5—C4—C8—C3 99.4 (2) N25'—C26'—C27'—C32' 134.3 (3)
N5—C4—C8—C7 −13.8 (3) C22'—C26'—C27'—C28' 128.7 (3)
N5—C6—C7—C8 −7.4 (3) C22'—C26'—C27'—C32' −50.8 (4)
O44—C6—C7—C1 58.3 (3) C26'—C27'—C28'—C29' 179.9 (4)
O44—C6—C7—C8 172.6 (2) C32'—C27'—C28'—C29' −0.6 (6)
N5—C6—C7—C1 −121.8 (2) C26'—C27'—C32'—C31' −177.3 (3)
C1—C7—C8—C3 11.4 (3) C28'—C27'—C32'—C31' 3.1 (5)
C1—C7—C8—C4 129.6 (2) C27'—C28'—C29'—C30' −3.0 (7)
C6—C7—C8—C3 −105.6 (2) C28'—C29'—C30'—Cl1' −176.5 (4)
C6—C7—C8—C4 12.6 (2) C28'—C29'—C30'—C31' 4.2 (7)
N2—C9—C10—C15 29.6 (4) Cl1'—C30'—C31'—C32' 178.9 (3)
N2—C9—C10—C11 −153.3 (3) C29'—C30'—C31'—C32' −1.8 (6)
C15—C10—C11—C12 −0.4 (5) C30'—C31'—C32'—C27' −2.0 (6)
C9—C10—C11—C12 −177.7 (3) N24'—C33'—C34'—C35' −179.4 (4)
C9—C10—C15—C14 177.1 (3) C38'—C33'—C34'—C35' −2.1 (6)
C11—C10—C15—C14 −0.1 (4) N24'—C33'—C38'—C37' −179.4 (4)
C10—C11—C12—C13 1.0 (6) C34'—C33'—C38'—C37' 3.3 (6)
C11—C12—C13—C14 −1.1 (6) C33'—C34'—C35'—C36' −1.5 (7)
C12—C13—C14—C15 0.5 (5) C34'—C35'—C36'—C37' 3.7 (7)
C13—C14—C15—C10 0.1 (5) C35'—C36'—C37'—C38' −2.5 (7)
N5—C16—C17—C18 −176.6 (3) C36'—C37'—C38'—C33' −1.0 (7)