Table 3.
Operational Condition of TDU-GC/PFPD for Reduced Sulfur Compounds.
TDU | GC/PFPD | |||
---|---|---|---|---|
Cold trap packing | Carbopack B+Silica Gel | Carrier gas | N2 | |
flow | Column | 20 psi | ||
Air (1) | 10 mL/min | |||
Air (2) | 10 mL/min | |||
H2 | 11.5 mL/min | |||
Adsorption flow | 5∼10 mL/min | GC Column | BP-1 (60 m × 0.32 mm, 5.0 um) | |
Cold trap high temp. | 300 °C | |||
Cold trap low temp. | -15 °C | Oven Temp. | 40 °C (10min) − 5 °C/min | |
Hold time | 5.0 min | |||
Outlet split | 5.0 mL/min(5:1 split ratio) | - 200 °C (5min) | ||
Flow path temp. | 80 °C |