| Bruker APEX DUO CCD area-detector diffractometer | 2379 independent reflections |
| Radiation source: sealed tube | 2073 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.040 |
| φ and ω scans | θmax = 72.1°, θmin = 4.6° |
| Absorption correction: multi-scan (SADABS; Bruker, 2009) | h = −11→12 |
| Tmin = 0.445, Tmax = 0.746 | k = −9→9 |
| 15551 measured reflections | l = −19→18 |