| Enraf–Nonius CAD-4 diffractometer | 2784 reflections with I > 2σ(I) |
| Radiation source: fine-focus sealed tube | Rint = 0.058 |
| Graphite monochromator | θmax = 25.3°, θmin = 1.1° |
| ω/2θ scans | h = −14→13 |
| Absorption correction: ψ scan (North et al., 1968) | k = 0→11 |
| Tmin = 0.957, Tmax = 0.978 | l = 0→23 |
| 4180 measured reflections | 3 standard reflections every 200 reflections |
| 3977 independent reflections | intensity decay: 1% |
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