Nonius KappaCCD diffractometer | 2183 reflections with I > 2σ(I) |
Radiation source: fine-focus sealed tube | Rint = 0.085 |
Graphite monochromator | θmax = 27.5°, θmin = 1.7° |
Detector resolution: 9.1 pixels mm-1 | h = −35→36 |
ω scans at fixed χ = 55° | k = −8→9 |
26416 measured reflections | l = −26→25 |
3790 independent reflections |