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. 2012 Feb 17;68(Pt 3):o731. doi: 10.1107/S1600536812005831
Nonius KappaCCD diffractometer 2183 reflections with I > 2σ(I)
Radiation source: fine-focus sealed tube Rint = 0.085
Graphite monochromator θmax = 27.5°, θmin = 1.7°
Detector resolution: 9.1 pixels mm-1 h = −35→36
ω scans at fixed χ = 55° k = −8→9
26416 measured reflections l = −26→25
3790 independent reflections