Oxford Xcalibur Atlas Gemini diffractometer | 1873 independent reflections |
Graphite monochromator | 1736 reflections with I > 2σ(I) |
Detector resolution: 10.4685 pixels mm-1 | Rint = 0.037 |
ω scans | θmax = 26.1°, θmin = 3.7° |
Absorption correction: analytical (CrysAlis PRO; Oxford Diffraction, 2002) | h = −7→7 |
Tmin = 0.895, Tmax = 0.976 | k = −10→11 |
6356 measured reflections | l = −18→21 |