| Stoe IPDS 2T diffractometer | 3150 independent reflections |
| Radiation source: fine-focus sealed tube | 3038 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.066 |
| ω scans | θmax = 29.2°, θmin = 2.3° |
| Absorption correction: numerical (X-SHAPE and X-RED32; Stoe & Cie, 2002) | h = −7→7 |
| Tmin = 0.887, Tmax = 0.923 | k = −13→13 |
| 6589 measured reflections | l = −15→16 |
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