| Rigaku R-AXIS RAPID diffractometer | 4963 independent reflections |
| Radiation source: fine-focus sealed tube | 4776 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.035 |
| Detector resolution: 0 pixels mm-1 | θmax = 27.5°, θmin = 3.2° |
| ω scans | h = −23→23 |
| Absorption correction: multi-scan (ABSCOR; Higashi, 1995) | k = −8→8 |
| Tmin = 0.177, Tmax = 0.321 | l = −24→22 |
| 20300 measured reflections |
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