O1—C7 | 1.327 (3) | C10—H10A | 0.9800 |
O1—H1 | 0.858 (10) | C10—H10B | 0.9800 |
O2—C11 | 1.298 (3) | C10—H10C | 0.9800 |
N1—C7 | 1.354 (3) | C11—C12 | 1.423 (3) |
N1—N2 | 1.400 (2) | C12—C13 | 1.381 (3) |
N1—C1 | 1.417 (3) | C12—H12 | 0.9500 |
N2—C9 | 1.322 (3) | C13—C14 | 1.496 (3) |
N3—C13 | 1.356 (3) | C14—H14A | 0.9800 |
N3—C15 | 1.411 (3) | C14—H14B | 0.9800 |
N3—H2 | 0.888 (10) | C14—H14C | 0.9800 |
C1—C6 | 1.393 (3) | C15—C20 | 1.393 (3) |
C1—C2 | 1.395 (3) | C15—C16 | 1.398 (3) |
C2—C3 | 1.389 (3) | C16—C17 | 1.382 (3) |
C2—H2A | 0.9500 | C16—H16 | 0.9500 |
C3—C4 | 1.385 (3) | C17—C18 | 1.393 (3) |
C3—H3 | 0.9500 | C17—H17 | 0.9500 |
C4—C5 | 1.390 (3) | C18—C19 | 1.398 (3) |
C4—H4 | 0.9500 | C18—C21 | 1.498 (3) |
C5—C6 | 1.387 (3) | C19—C20 | 1.386 (3) |
C5—H5 | 0.9500 | C19—H19 | 0.9500 |
C6—H6 | 0.9500 | C20—H20 | 0.9500 |
C7—C8 | 1.396 (3) | C21—H21 | 0.9800 |
C8—C9 | 1.422 (3) | C21—H21B | 0.9800 |
C8—C11 | 1.441 (3) | C21—H21C | 0.9800 |
C9—C10 | 1.496 (3) | ||
C7—O1—H1 | 101 (3) | H10B—C10—H10C | 109.5 |
C7—N1—N2 | 109.97 (18) | O2—C11—C12 | 121.6 (2) |
C7—N1—C1 | 131.08 (18) | O2—C11—C8 | 116.39 (19) |
N2—N1—C1 | 118.94 (18) | C12—C11—C8 | 122.0 (2) |
C9—N2—N1 | 105.72 (18) | C13—C12—C11 | 125.9 (2) |
C13—N3—C15 | 130.94 (19) | C13—C12—H12 | 117.1 |
C13—N3—H2 | 111.0 (16) | C11—C12—H12 | 117.1 |
C15—N3—H2 | 117.1 (16) | N3—C13—C12 | 120.0 (2) |
C6—C1—C2 | 120.0 (2) | N3—C13—C14 | 120.3 (2) |
C6—C1—N1 | 118.77 (19) | C12—C13—C14 | 119.61 (19) |
C2—C1—N1 | 121.2 (2) | C13—C14—H14A | 109.5 |
C3—C2—C1 | 119.1 (2) | C13—C14—H14B | 109.5 |
C3—C2—H2A | 120.4 | H14A—C14—H14B | 109.5 |
C1—C2—H2A | 120.4 | C13—C14—H14C | 109.5 |
C4—C3—C2 | 121.2 (2) | H14A—C14—H14C | 109.5 |
C4—C3—H3 | 119.4 | H14B—C14—H14C | 109.5 |
C2—C3—H3 | 119.4 | C20—C15—C16 | 118.0 (2) |
C3—C4—C5 | 119.2 (2) | C20—C15—N3 | 125.0 (2) |
C3—C4—H4 | 120.4 | C16—C15—N3 | 117.0 (2) |
C5—C4—H4 | 120.4 | C17—C16—C15 | 120.9 (2) |
C6—C5—C4 | 120.4 (2) | C17—C16—H16 | 119.5 |
C6—C5—H5 | 119.8 | C15—C16—H16 | 119.5 |
C4—C5—H5 | 119.8 | C16—C17—C18 | 121.6 (2) |
C5—C6—C1 | 120.0 (2) | C16—C17—H17 | 119.2 |
C5—C6—H6 | 120.0 | C18—C17—H17 | 119.2 |
C1—C6—H6 | 120.0 | C17—C18—C19 | 117.1 (2) |
O1—C7—N1 | 125.3 (2) | C17—C18—C21 | 121.2 (2) |
O1—C7—C8 | 126.2 (2) | C19—C18—C21 | 121.6 (2) |
N1—C7—C8 | 108.45 (19) | C20—C19—C18 | 121.8 (2) |
C7—C8—C9 | 104.0 (2) | C20—C19—H19 | 119.1 |
C7—C8—C11 | 119.7 (2) | C18—C19—H19 | 119.1 |
C9—C8—C11 | 136.3 (2) | C19—C20—C15 | 120.5 (2) |
N2—C9—C8 | 111.87 (19) | C19—C20—H20 | 119.7 |
N2—C9—C10 | 119.0 (2) | C15—C20—H20 | 119.7 |
C8—C9—C10 | 129.1 (2) | C18—C21—H21 | 109.5 |
C9—C10—H10A | 109.5 | C18—C21—H21B | 109.5 |
C9—C10—H10B | 109.5 | H21—C21—H21B | 109.5 |
H10A—C10—H10B | 109.5 | C18—C21—H21C | 109.5 |
C9—C10—H10C | 109.5 | H21—C21—H21C | 109.5 |
H10A—C10—H10C | 109.5 | H21B—C21—H21C | 109.5 |
C7—N1—N2—C9 | −0.2 (2) | C11—C8—C9—N2 | −178.4 (2) |
C1—N1—N2—C9 | 178.60 (16) | C7—C8—C9—C10 | 179.3 (2) |
C7—N1—C1—C6 | −180.0 (2) | C11—C8—C9—C10 | 1.1 (4) |
N2—N1—C1—C6 | 1.5 (3) | C7—C8—C11—O2 | −0.3 (3) |
C7—N1—C1—C2 | −0.1 (3) | C9—C8—C11—O2 | 177.8 (2) |
N2—N1—C1—C2 | −178.62 (17) | C7—C8—C11—C12 | −179.00 (18) |
C6—C1—C2—C3 | 0.1 (3) | C9—C8—C11—C12 | −1.0 (4) |
N1—C1—C2—C3 | −179.74 (17) | O2—C11—C12—C13 | −3.5 (3) |
C1—C2—C3—C4 | 0.4 (3) | C8—C11—C12—C13 | 175.14 (19) |
C2—C3—C4—C5 | −0.2 (3) | C15—N3—C13—C12 | −172.5 (2) |
C3—C4—C5—C6 | −0.5 (3) | C15—N3—C13—C14 | 5.7 (3) |
C4—C5—C6—C1 | 1.0 (3) | C11—C12—C13—N3 | 0.9 (3) |
C2—C1—C6—C5 | −0.8 (3) | C11—C12—C13—C14 | −177.35 (18) |
N1—C1—C6—C5 | 179.08 (17) | C13—N3—C15—C20 | −36.1 (3) |
N2—N1—C7—O1 | 179.73 (18) | C13—N3—C15—C16 | 146.9 (2) |
C1—N1—C7—O1 | 1.1 (3) | C20—C15—C16—C17 | −0.6 (3) |
N2—N1—C7—C8 | 0.1 (2) | N3—C15—C16—C17 | 176.58 (19) |
C1—N1—C7—C8 | −178.55 (18) | C15—C16—C17—C18 | 1.6 (3) |
O1—C7—C8—C9 | −179.57 (19) | C16—C17—C18—C19 | −1.0 (3) |
N1—C7—C8—C9 | 0.1 (2) | C16—C17—C18—C21 | −178.35 (19) |
O1—C7—C8—C11 | −1.0 (3) | C17—C18—C19—C20 | −0.6 (3) |
N1—C7—C8—C11 | 178.65 (17) | C21—C18—C19—C20 | 176.7 (2) |
N1—N2—C9—C8 | 0.3 (2) | C18—C19—C20—C15 | 1.7 (3) |
N1—N2—C9—C10 | −179.30 (17) | C16—C15—C20—C19 | −1.0 (3) |
C7—C8—C9—N2 | −0.2 (2) | N3—C15—C20—C19 | −177.94 (19) |