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. Author manuscript; available in PMC: 2013 Mar 5.
Published in final edited form as: Inorg Chem. 2012 Feb 23;51(5):2917–2929. doi: 10.1021/ic2021726

Figure 5.

Figure 5

EPR spectra of 1 in PrCN in the low field region recorded at T = 8 K (green), 21 K (blue) and 34 K (red). The blue line in the lower trace is a simulation of the 34 K spectrum with eq 1, using the parameters listed in Table 4. To simulate the approximate line shape, EB/DB was assumed to have a Gaussian distribution with σE/D = 0.04. The feature at g = 4.3 is due to a minor S = 5/2 contaminant. Conditions: 9.62 GHz, 0.2 mW microwave power, 1 mT modulation; 1 hour accumulation time for the 34 K spectrum.