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. Author manuscript; available in PMC: 2013 Mar 15.
Published in final edited form as: J Chromatogr B Analyt Technol Biomed Life Sci. 2012 Feb 13;889-890:110–115. doi: 10.1016/j.jchromb.2012.02.005

Table 3.

Accuracy and precision of the etheno-adenine nucleotide analysis

Adenine nucleotide Theoretical Value (pmol) Experimental valuea (pmol) Error (%) Precision (RSD, %)
Intra-dayb Inter-daya
adenosine 10.3 10.6±0.3 2.5 1.5 3.3
5.2 5.6±0.2 7.9 1.6 2.8
1.6 1.6±0.0 1.7 1.6 2.9

AMP 10.3 10.0±0.2 −3.3 0.6 2.4
5.2 5.2±0.1 1.8 1.5 2.4
1.6 1.6±0.1 6.4 3.7 3.1

ADP 9.6 9.3±0.2 −3.5 5.1 2.6
4.8 4.7±0.1 −3.0 2.3 2.0
1.4 1.4±0.0 −1.1 4.3 1.9

ATP 9.8 8.7±0.2 −11.0 1.8 2.9
4.9 4.2±0.1 −13.4 2.9 3.4
1.5 1.3±0.0 −12.2 3.2 0.6
a

nine replicates

b

three replicates