Table 3.
Accuracy and precision of the etheno-adenine nucleotide analysis
| Adenine nucleotide | Theoretical Value (pmol) | Experimental valuea (pmol) | Error (%) | Precision (RSD, %)
|
|
|---|---|---|---|---|---|
| Intra-dayb | Inter-daya | ||||
| adenosine | 10.3 | 10.6±0.3 | 2.5 | 1.5 | 3.3 |
| 5.2 | 5.6±0.2 | 7.9 | 1.6 | 2.8 | |
| 1.6 | 1.6±0.0 | 1.7 | 1.6 | 2.9 | |
|
| |||||
| AMP | 10.3 | 10.0±0.2 | −3.3 | 0.6 | 2.4 |
| 5.2 | 5.2±0.1 | 1.8 | 1.5 | 2.4 | |
| 1.6 | 1.6±0.1 | 6.4 | 3.7 | 3.1 | |
|
| |||||
| ADP | 9.6 | 9.3±0.2 | −3.5 | 5.1 | 2.6 |
| 4.8 | 4.7±0.1 | −3.0 | 2.3 | 2.0 | |
| 1.4 | 1.4±0.0 | −1.1 | 4.3 | 1.9 | |
|
| |||||
| ATP | 9.8 | 8.7±0.2 | −11.0 | 1.8 | 2.9 |
| 4.9 | 4.2±0.1 | −13.4 | 2.9 | 3.4 | |
| 1.5 | 1.3±0.0 | −12.2 | 3.2 | 0.6 | |
nine replicates
three replicates