Table 4.
Position | δC (ppm) | δH mult (J in Hz) |
---|---|---|
1 | 45.0 | 3.77 t (7) |
2 | 24.5 | 2.14 ddt (7, 8, 8) |
3α | 51.4 | 2.96 dt (8, 13.5) |
3β | 51.4 | 2.84 dt (8, 13.5) |
4 | 38.2 | 2.68 s |
5 | 132.8 |
Recorded in CDCl3. δC, carbon chemical shift value; δH, proton chemical shift value; mult, multiplicity of proton NMR peaks; J, coupling constant(s) in hertz (Hz).