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. Author manuscript; available in PMC: 2012 Jun 21.
Published in final edited form as: Org Biomol Chem. 2011 Mar 21;9(12):4444–4447. doi: 10.1039/c1ob05052d

Table 1.

H-bonding parameters (Å, °) for the bisulfate complex of L

D—H ··· O H ··· O D ··· O ∠DHO
O1—H1A ··· O20a 1.79(3) 2.573(2) 178(3)
N4—H4 ··· O3b 2.15(3) 2.979(3) 169(2)
N7—H7 ··· O2b 2.12(3) 2.936(3) 171(2)
N18—H18 ··· O1 2.23(2) 2.981(2) 159(2)
N21—H21 ··· O1 2.20(2) 3.020(3) 153(2)
N32—H32 ··· O4a 2.40(2) 3.092(3) 142(2)
N35—H35 ··· O4a 2.06(3) 2.857(3) 170(2)
a

12x,12+y,12z,

b

12x,12+y,12z.