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. 2011 Nov 17;(57):3399. doi: 10.3791/3399
Mass Spectrometry Parameter Setting
Source APCI
Mode Negative Ion
Method Length 40 min
MRM Scan Width 0.002 m/z
MRM Scan Time 0.15 sec
MRM Peak Width 0.70 FWHM
Tube Lens 164 V
Source CID 10 eV
Q2 Collision Gas 1.5 units
Vaporizer Temperature 450°C
Capillary Temperature 250°C
Discharge Current 0 μA
Sheath Gas Pressure 25 units
Ion Sweep Pressure 3 units
Auxiliary Gas Pressure 5 units