Table 1. Data-collection statistics.
| Peak | Inflection | Remote | Remote wedge (290–430°) | |
|---|---|---|---|---|
| Space group | P41212 | |||
| Unit-cell parameters (Å, °) | a = b = 66.25, c = 129.37, α = β = γ = 90.00 | |||
| Molecules per asymmetric unit | 1 | |||
| Matthews coefficient (Å3 Da−1) | 2.75 | |||
| Solvent content (%) | 55.4 | |||
| Resolution (Å) | 59–2.34 (2.47–2.34) | 59–2.34 (2.47–2.34) | 59–2.34 (2.47–2.34) | 46.9–2.15 (2.27–2.15) |
| Wavelength (Å) | 0.9800 | 0.9802 | 0.9537 | 0.9537 |
| Mosaicity (°) | 0.67 | 0.69 | 0.70 | 0.67 |
| Rmerge | 0.158 (0.707) | 0.149 (0.509) | 0.163 (0.611) | 0.100 (0.627) |
| Rmeas (within I+/I−) | 0.164 (0.736) | 0.155 (0.529) | 0.169 (0.632) | 0.111 (0.695) |
| Observed reflections | 238848 (39070) | 332088 (41035) | 339770 (50988) | 84566 (12492) |
| Unique reflections | 12618 (1618) | 12610 (1620) | 12830 (1842) | 16317 (2316) |
| Mean I/σ(I) | 14.6 (4.5) | 15.3 (5.6) | 14.1 (5.2) | 7.9 (2.1) |
| Completeness (%) | 99.7 (98.4) | 99.8 (99.8) | 99.8 (100) | 99.6 (100) |
| Multiplicity | 26.1 (24.1) | 26.3 (25.3) | 26.5 (27.7) | 5. 2 (5.4) |
| Anomalous completeness (%) | 99.7 (98.3) | 99.9 (99.8) | 99.9 (100) | 99.2 (99.3) |
| Anomalous multiplicity | 14.4 (12.9) | 14.6 (13.5) | 14.6 (14.9) | 2.8 (2.8) |