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. Author manuscript; available in PMC: 2013 Feb 6.
Published in final edited form as: Chemistry. 2012 Jan 11;18(6):1711–1726. doi: 10.1002/chem.201101703

Table 1.

Aminooxygenation reaction of N-tosyl-o-allylaniline using different solvents and bases.

graphic file with name nihms362192u2.jpg
Entry Solvent Base Yield [%][a]
1 CF3Ph Cs2CO3 85
2 CH3Ph Cs2CO3 87
3 xylenes Cs2CO3 90
4 CH3Ph proton sponge 57
5 CH3Ph NBu4OAc 96
6 CH3Ph 2,5-di-tBu-4-Me-pyridine 83
7 CH3Ph – 70
[a]

Yield refers to amount of 2 isolated after flash chromatography.